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مقاله Nanoporous Hydrogel Based on Polysaccharide/ Protein Hybrid Backbone: Synthesis and Characterization word دارای 3 صفحه می باشد و دارای تنظیمات در microsoft word می باشد و آماده پرینت یا چاپ است

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بخشی از متن مقاله Nanoporous Hydrogel Based on Polysaccharide/ Protein Hybrid Backbone: Synthesis and Characterization word :

سال انتشار: 1388

محل انتشار: سومین کنفرانس نانوساختارها

تعداد صفحات: 3

نویسنده(ها):

A Pourjavadi – Department of Chemistry, Sharif University of Technology, P.O. Box 11365-9516, Iran
R Soleyman – Department of Chemistry, Sharif University of Technology, P.O. Box 11365-9516, Iran
G.R Bardajee – Department of Chemistry, Payame Noor University, Qazvin Branch, Qazvin, Iran,

چکیده:

A novel high capacity swelling NanoPorous Hydrogel (NPH) was synthesized via graft copolymerization of acrylamide (AAm) onto kappa-Carrageenan (kC, as a polysaccharide) and gelatin (as a protein) hybrid backbone, after hydrolysis of this system. The Taguchi method as a strong experimental design tool was used for its optimized synthesis. The Taguchi method was applied for the experimental and standard 9 orthogonal array (OA) with four factors and three levels for each factor. A series of NPHs were synthesized by proposed conditions of Qualitek-4
Software. Considering the results of 9 trials according to analysis of variance (ANOVA), optimum conditions were proposed. The swelling behavior of optimum NPHs was measured in various solutions with pH values ranging from 1 to 13. In addition, swelling kinetics, swelling in various organic solvents and various salt solutions were investigated. The hydrogel formation was confirmed by Fourier transform infrared spectroscopy (FTIR) and thermogravimetrical analysis (TGA). The study of the surface morphology of hydrogels using SEM showed a highly nanoporous and cellular structure for the sample obtained under optimized condition.

 

 

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